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Determination of 27 pharmaceuticals and personal care products (PPCPs) in water: The benefit of isotope dilution

Xueqi Fan, Jie Gao, Wenchao Li, Jun Huang, Gang Yu

《环境科学与工程前沿（英文）》 2020年 第14卷 第1期 doi: 10.1007/s11783-019-1187-3

摘要： • Isotope dilution method was developed for the determination of 27 PPCPs in water. • The established method was successfully applied to different types of water samples. • The correction effect of corresponding 27 ILSs over 70 d was investigated. • Benefit of isotopic dilution method was illustrated for three examples. Pharmaceuticals and personal care products (PPCPs) are a unique group of emerging and non-persistent contaminants. In this study, 27 PPCPs in various water samples were extracted by solid phase extraction (SPE), and determined by isotope dilution method using liquid chromatography coupled to tandem triple quadruple mass spectrometer (LC-MS/MS). A total of 27 isotopically labeled standards (ILSs) were applied to correct the concentration of PPCPs in spiked ultrapure water, drinking water, river, effluent and influent sewage. The corrected recoveries were 73%–122% with the relative standard deviation (RSD)<16%, except for acetaminophen. The matrix effect for all kinds of water samples was<22% and the method quantitation limits (MQLs) were 0.45–8.6 ng/L. The developed method was successfully applied on environmental water samples. The SPE extracts of spiked ultrapure water, drinking water, river and wastewater effluent were stored for 70 days, and the ILSs-corrected recoveries of 27 PPCPs were obtained to evaluate the correction ability of ILSs in the presence of variety interferences. The recoveries of 27 PPCPs over 70 days were within the scope of 72%–140% with the recovery variation<37% in all cases. The isotope dilution method seems to be of benefit when the extract has to be stored for long time before the instrument analysis.

关键词： Pharmaceuticals and personal care products (PPCPs)     Isotopically labeled standard (ILSs)     Water     Solid-phase extraction (SPE)     LC-MS/MS    

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p-type transition metal dichalcogenide used for the detection of ultra-trace amounts of diclofenac via a labeled

Abdolhamid Hatefi-Mehrjardi, Amirkhosro Beheshti-Marnani, Zarrin Es'haghi

《化学科学与工程前沿（英文）》 2019年 第13卷 第4期   页码 823-831 doi: 10.1007/s11705-019-1797-0

摘要： A -type transition metal dichalcogenide (WS ) was synthesized and hybridized with graphene oxide via a simple hydrothermal method. The as-prepared material was used to modify a glassy carbon electrode for the fabrication of a simple, stable, and repeatable methylene blue-labeled “signal-off” aptasensor used for the sensitive determination of very low amounts of sodium diclofenac (DCF). The synthetic material, modification process, and role of WS in the current response enhancement were studied by X-ray diffraction, energy-dispersive X-ray spectroscopy, field emission scanning electron microscopy, high resolution transmission electron microscopy, Hall effect, cyclic voltammetry, differential pulse voltammetry, and electrochemical impedance spectroscopy. Subsequently, a wide linear range of DCF concentration (0.5–300 nmol/L), very low limit of detection (0.23 nmol/L), and good selectivity were obtained using the differential pulse voltammetry method with the assembled aptasensor. Finally, the fabricated aptasensor was successfully developed for physiological real samples with significant recoveries.

关键词： labeled aptasensor     transition metal dichalcogenide     graphene oxide     sodium diclofenac    

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Research on the ecological compensation standard of the basin pollution control project based on evolutionary

Dongbin HU, Huiwu LIU, Xiaohong CHEN, Yang CHEN

《工程管理前沿（英文）》 2019年 第6卷 第4期   页码 575-583 doi: 10.1007/s42524-019-0044-1

摘要： Ecological compensation is a new resource and environment management model. As one of the main areas for implementing ecological compensation policies, basin ecological compensation has become an important measure for encouraging basin pollution control projects and improving the quality of regional economic development. By applying the basic game analysis of evolutionary game theory and building an evolutionary game model with a “reward–punishment” mechanism, this paper compares the interest-related decision-making behaviors of the upstream and downstream stakeholders of basin ecological compensation. By using data on the water quality of Xiangjiang River Basin, this paper calculates the rewards and penalties in different intervals by building a parametric regression mathematical model and employing the local linear regression method. Results show that a decline in water quality should be fined RMB 925500 yuan, an improvement in water quality should be awarded RMB 1227800 yuan, and a deteriorating water quality should be severely fined RMB 5087600 yuan.

关键词： evolutionary game     ecological compensation standard     Xiangjiang River Basin    

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transporter and vesicular monoamine transporter 2 genes for increased retention of metaiodobenzylguanidine labeled

null

《医学前沿（英文）》 2017年 第11卷 第1期   页码 120-128 doi: 10.1007/s11684-017-0501-3

摘要：

Norepinephrine transporter (NET) transfection leads to significant uptake of iodine-131-labeled metaiodobenzylguanidine (131I-MIBG) in non-neuroendocrine tumors. However, the use of 131I-MIBG is limited by its short retention time in target cells. To prolong the retention of 131I-MIBG in target cells, we infected hepatocarcinoma (HepG2) cells with Lentivirus-encoding human NET and vesicular monoamine transporter 2 (VMAT2) genes to obtain NET-expressing, NET-VMAT2-coexpressing, and negative-control cell lines. We evaluated the uptake and efflux of 131I-MIBG both in vitro and in vivo in mice bearing transfected tumors. NET-expressing and NET-VMAT2-coexpressing cells respectively showed 2.24 and 2.22 times higher 131I-MIBG uptake than controls. Two hours after removal of 131I-MIBG-containing medium, 25.4% efflux was observed in NET-VMAT2-coexpressing cells and 38.6% in NET-expressing cells. In vivo experiments were performed in nude mice bearing transfected tumors; results revealed that NET-VMAT2-coexpressing tumors had longer 131I-MIBG retention time than NET-expressing tumors. Meanwhile, NET-VMAT2-coexpressing and NET-expressing tumors displayed 0.54% and 0.19%, respectively, of the injected dose per gram of tissue 24 h after 131I-MIBG administration. Cotransfection of HepG2 cells with NET and VMAT2resulted in increased 131I-MIBG uptake and retention. However, the degree of increase was insufficient to be therapeutically effective in target cells.

关键词： norepinephrine transporter     vesicular monoamine transporter 2     -MIBG     gene therapy     lentivirus vector    

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Standard model of knowledge representation

Wensheng YIN

《机械工程前沿（英文）》 2016年 第11卷 第3期   页码 275-288 doi: 10.1007/s11465-016-0372-3

摘要：

Knowledge representation is the core of artificial intelligence research. Knowledge representation methods include predicate logic, semantic network, computer programming language, database, mathematical model, graphics language, natural language, etc. To establish the intrinsic link between various knowledge representation methods, a unified knowledge representation model is necessary. According to ontology, system theory, and control theory, a standard model of knowledge representation that reflects the change of the objective world is proposed. The model is composed of input, processing, and output. This knowledge representation method is not a contradiction to the traditional knowledge representation method. It can express knowledge in terms of multivariate and multidimensional. It can also express process knowledge, and at the same time, it has a strong ability to solve problems. In addition, the standard model of knowledge representation provides a way to solve problems of non-precision and inconsistent knowledge.

关键词： knowledge representation     standard model     ontology     system theory     control theory     multidimensional representation    

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Overview of the quality standard research of traditional Chinese medicine

Huimin Gao, Zhimin Wang, Yujuan Li, Zhongzhi Qian

《医学前沿（英文）》 2011年 第5卷 第2期   页码 195-202 doi: 10.1007/s11684-011-0134-x

摘要： Traditional Chinese medicine (TCM) has been widely used for the prevention and treatment of various diseases for a long time in China. Due to its proven efficacy, wide applications, and low side effect, TCM has increasingly attracted worldwide attention. However, one of the biggest challenges facing the clinical practice of TCM is the uncontrollable quality. In this review, the progress of the development and the current status of quality standard as well as new quality control techniques introduced in (2010 edition), such as liquid chromatography hyphenated mass spectrometry (LC-MS), fingerprint, quantitative analysis of multi-components by single-marker (QAMS), thin layer chromatography bio-autographic assay (TLC-BAA), and DNA molecular marker technique, are briefly overviewed.

关键词： traditional Chinese medicine     quality standard     quality control     quantitative analysis of multi-components by single-marker    

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A Standard for the Commissioning Process

William L. Gillis,Elizabeth A. Cudney

《工程管理前沿（英文）》 2015年 第2卷 第1期   页码 39-51 doi: 10.15302/J-FEM-2015006

摘要： The demand for commissioning services for new-building construction projects is experiencing rapid growth. Commissioning (Cx) is touted as being a quality-focused process for ensuring the owner’s project requirements (OPR) are met by design, final construction, and the operations of a building. To an owner this is just what is needed to receive a perfect building at occupancy. However, as many owners have realized, the Cx process does not guarantee the completed building will be what was expected. It should be pointed out that this is typically not caused by the Cx process, but the Cx process should or could have identified, in the early phases of the project, many of the issues that made it through to the completed building. There are a number of reasons why the Cx services received may not be optimal. Often it is poor communication and the transfer of knowledge between project teams. Cx should and can facilitate both communication and the transfer of knowledge from phase to phase. An adaptation of the quality function deployment (QFD) four-phase model can accomplish this by filling the gaps among the major Cx activities and provide a standard approach to the process. The four-phase model effectively links each of the Cx activities to each other and back to the OPR, providing a method for improved communication and knowledge transfer. This paper investigates some potential reasons for inconsistent Cx services, presents an argument for the need of a Cx standard, and proposes a potential standard.

关键词： construction     engineering management     quality     commissioning    

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State identification of home appliance with transient features in residential buildings

《能源前沿（英文）》 2022年 第16卷 第1期   页码 130-143 doi: 10.1007/s11708-022-0822-z

摘要： Nonintrusive load monitoring (NILM) is crucial for extracting patterns of electricity consumption of household appliance that can guide users’ behavior in using electricity while their privacy is respected. This study proposes an online method based on the transient behavior of individual appliances as well as system steady-state characteristics to estimate the operating states of the appliances. It determines the number of states for each appliance using the density-based spatial clustering of applications with noise (DBSCAN) method and models the transition relationship among different states. The states of the working appliances are identified from aggregated power signals using the Kalman filtering method in the factorial hidden Markov model (FHMM). Thereafter, the identified states are confirmed by the verification of system states, which are the combination of the working states of individual appliances. The verification step involves comparing the total measured power consumption with the total estimated power consumption. The use of transient features can achieve fast state inference and it is suitable for online load disaggregation. The proposed method was tested on a high-resolution data set such as Labeled hIgh-Frequency daTaset for Electricity Disaggregation (LIFTED) and it outperformed other related methods in the literature.

关键词： nonintrusive load monitoring (NILM)     load disaggregation     online load disaggregation     Kalman filtering     factorial hidden Markov model (FHMM)     Labeled hIgh-Frequency daTaset for Electricity Disaggregation (LIFTED)    

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Quantitative standard of eco-compensation for the water source area in the middle route of the South-to-North

Zhanfeng DONG, Jinnan WANG

《环境科学与工程前沿（英文）》 2011年 第5卷 第3期   页码 459-473 doi: 10.1007/s11783-010-0288-9

摘要： The Middle Route Project(MRP) of the South-to-North Water Transfer Scheme (SNWT) in China will require a very large financial expenditure to ensure the water supply and the associated water quality to northern China. An eco-compensation mechanism between the water service source areas and its beneficiaries is essential. This paper establishes an analytic framework of eco-compensation standard for the protection of the water source area, including both the calculation of eco-compensation based on opportunity cost method (OCM) and calculation of the burden sharing of eco-compensation between the water source area and the external water reception area based on the deviation square method (DSM). Taking Shiyan City, Hubei Province in China as a case study, our results show that the eco-compensation in the first-phase of MRP for the water source area in Shiyan, Hubei Province should be 1.63×10 CNY, about four times of planned eco-construction investment budget(4.33×10 CNY). In addition, the burden sharing of eco-compensation varied greatly in terms of different methods. It would be better to integrate the results of different single-factor burden sharing methods by determining the corresponding weighting coefficient with DSM and form one unanimous consent result by the interested parties.

关键词： the South-to-North Water Transfer Scheme     eco-compensation standard     opportunity costs     deviation square method    

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Optimization of the power, efficiency and ecological function for an air-standard irreversible Dual-Miller

Zhixiang WU, Lingen CHEN, Yanlin GE, Fengrui SUN

《能源前沿（英文）》 2019年 第13卷 第3期   页码 579-589 doi: 10.1007/s11708-018-0557-z

摘要： This paper establishes an irreversible Dual-Miller cycle (DMC) model with the heat transfer (HT) loss, friction loss (FL) and other internal irreversible losses. To analyze the effects of the cut-off ratio ( ) and Miller cycle ratio ( ) on the power output ( ), thermal efficiency ( ) and ecological function ( ), obtain the optimal and optimal , and compare the performance characteristics of DMC with its simplified cycles and with different optimization objective functions, the , and of irreversible DMC are analyzed and optimized by applying the finite time thermodynamic (FTT) theory. Expressions of , and are derived. The relationships among , , and compression ratio ( ) are obtained by numerical examples. The effects of and on , , , maximum power output ( ), maximum efficiency ( ) and maximum ecological function ( ) are analyzed. Performance differences among the DMC, the Otto cycle (OC), the Dual cycle (DDC), and the Otto-Miller cycle (OMC) are compared for fixed design parameters. Performance characteristics of irreversible DMC with the choice of , and as optimization objective functions are analyzed and compared. The results show that the irreversible DMC engine can reach a twice-maximum power, a twice-maximum efficiency, and a twice-maximum ecological function, respectively. Moreover, when choosing as the optimization objective, there is a 5.2% of improvement in while there is a drop of only 2.7% in compared to choosing as the optimization objective. However, there is a 5.6% of improvement in while there is a drop of only 1.3% in compared to choosing as the optimization objective.

关键词： finite-time thermodynamics     Dual-Miller cycle     power output     thermal efficiency     ecological function    

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High-precision standard enthalpy of formation for polycyclic aromatic hydrocarbons predicting from general

《化学科学与工程前沿（英文）》 2022年 第16卷 第12期   页码 1743-1750 doi: 10.1007/s11705-022-2184-9

摘要： The standard enthalpy of formation is an important predictor of the reaction heat of a chemical reaction. In this work, a high-precision method was developed to calculate accurate standard enthalpies of formation for polycyclic aromatic hydrocarbons based on the general connectivity based hierarchy (CBH) with the discrete correction of atomization energy. Through a comparison with available experimental findings and other high-precision computational results, it was found that the present method can give a good description of enthalpy of formation for polycyclic aromatic hydrocarbons. Since CBH schemes can broaden the scope of application, this method can be used to investigate the energetic properties of larger polycyclic aromatic hydrocarbons to achieve a high-precision calculation at the CCSD(T)/CBS level. In addition, the energetic properties of CBH fragments can be accurately calculated and integrated into a database for future use, which will increase computational efficiency. We hope this work can give new insights into the energetic properties of larger systems.

关键词： standard enthalpy of formation     polycyclic aromatic hydrocarbons     connectivity based hierarchy     high-precision calculation    

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Punching of reinforced concrete slab without shear reinforcement: Standard models and new proposal

Luisa PANI, Flavio STOCHINO

《结构与土木工程前沿（英文）》 2020年 第14卷 第5期   页码 1196-1214 doi: 10.1007/s11709-020-0662-z

摘要： Reinforced concrete (RC) slabs are characterized by reduced construction time, versatility, and easier space partitioning. Their structural behavior is not straightforward and, specifically, punching shear strength is a current research topic. In this study an experimental database of 113 RC slabs without shear reinforcement under punching loads was compiled using data available in the literature. A sensitivity analysis of the parameters involved in the punching shear strength assessment was conducted, which highlighted the importance of the flexural reinforcement that are not typically considered for punching shear strength. After a discussion of the current international standards, a new proposed model for punching shear strength and rotation of RC slabs without shear reinforcement was discussed. It was based on a simplified load-rotation curve and new failure criteria that takes into account the flexural reinforcement effects. This experimental database was used to validate the approaches of the current international standards as well as the new proposed model. The latter proved to be a potentially useful design tool.

关键词： punching shear strength     reinforced concrete     slabs     reinforcement ratio    

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大庆油田A区块油气水层解释标准研究

徐通

《中国工程科学》 2012年 第14卷 第4期   页码 83-87

摘要：

利用A区块部分探井、评价井及开发井的试油、取心及测井资料，分析统计储层岩性、物性、含油性及电性这“四性”之间的关系，建立油气水层的电性解释标准。主要是利用旋转式井壁取心及钻井取心资料，分析统计储层的岩性、物性特征；利用取心井及试油井资料分析统计储层的油水层发育状况。利用图表法，得出岩性、物性及含油性之间的相关性。并把油气水层对应于不同的测井曲线值上，优选出符合率最高的曲线组合作为最终的解释标准，指导区块射孔方案的编制。

关键词： “四性”     取心     试油     测井     解释标准    

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AMMONIA DISPERSION FROM MULTI-FLOOR VERSUS STANDARD SINGLE-FLOOR PIG PRODUCTION FACILITIES BASED ON COMPUTATIONAL

《农业科学与工程前沿（英文）》 2023年 第10卷 第3期   页码 374-389 doi: 10.15302/J-FASE-2023501

摘要：

● NH3 dispersion from a multi-floor pig building was compared to a single-floor building.

关键词： pig building     computational fluid dynamics     ammonia     dispersion    

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prediction method of industrial atmospheric pollutant emission intensity based on pollutant emission standard

《环境科学与工程前沿（英文）》 2023年 第17卷 第1期 doi: 10.1007/s11783-023-1608-1

摘要：

● Established a quantification method of pollutant emission standard.

关键词： Industrial atmospheric pollutants     Pollutant emission standards     Quantitative method     Machine learning     Single enterprise    

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标题 作者 时间 类型 操作

Determination of 27 pharmaceuticals and personal care products (PPCPs) in water: The benefit of isotope dilution

Xueqi Fan, Jie Gao, Wenchao Li, Jun Huang, Gang Yu

期刊论文

p-type transition metal dichalcogenide used for the detection of ultra-trace amounts of diclofenac via a labeled

Abdolhamid Hatefi-Mehrjardi, Amirkhosro Beheshti-Marnani, Zarrin Es'haghi

期刊论文

Research on the ecological compensation standard of the basin pollution control project based on evolutionary

Dongbin HU, Huiwu LIU, Xiaohong CHEN, Yang CHEN

期刊论文

transporter and vesicular monoamine transporter 2 genes for increased retention of metaiodobenzylguanidine labeled

null

期刊论文

Standard model of knowledge representation

Wensheng YIN

期刊论文

Overview of the quality standard research of traditional Chinese medicine

Huimin Gao, Zhimin Wang, Yujuan Li, Zhongzhi Qian

期刊论文

A Standard for the Commissioning Process

William L. Gillis,Elizabeth A. Cudney

期刊论文

State identification of home appliance with transient features in residential buildings

期刊论文

Quantitative standard of eco-compensation for the water source area in the middle route of the South-to-North

Zhanfeng DONG, Jinnan WANG

期刊论文

Optimization of the power, efficiency and ecological function for an air-standard irreversible Dual-Miller

Zhixiang WU, Lingen CHEN, Yanlin GE, Fengrui SUN

期刊论文

High-precision standard enthalpy of formation for polycyclic aromatic hydrocarbons predicting from general

期刊论文

Punching of reinforced concrete slab without shear reinforcement: Standard models and new proposal

Luisa PANI, Flavio STOCHINO

期刊论文

大庆油田A区块油气水层解释标准研究

徐通

期刊论文

AMMONIA DISPERSION FROM MULTI-FLOOR VERSUS STANDARD SINGLE-FLOOR PIG PRODUCTION FACILITIES BASED ON COMPUTATIONAL

期刊论文

prediction method of industrial atmospheric pollutant emission intensity based on pollutant emission standard

期刊论文